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Beilstein J. Org. Chem. 2010, 6, 938–944, doi:10.3762/bjoc.6.105
Graphical Abstract
Scheme 1: One-pot synthesis of epoxide-amine adducts via MW-assisted transfer hydrogenation.
Figure 1: 13C NMR spectra of 4, measured in CDCl3.
Figure 2: MALDI-TOF MS spectra (linear mode) of epoxide-amine product 4.
Figure 3: GPC curve of epoxide-amine product 4 detected by UV absorption.
Figure 4: Number-average hydrodynamic diameters of compound 4 prepared via the one-pot (continuous line) and ...
Scheme 2: Ring-opening polymerization of ε-CL using alcohol units as initiator.
Figure 5: GPC curves of the new formed graft copolymer 6 detected by UV absorption (continuous line) and RI (...
Figure 6: Number-average hydrodynamic diameters of compounds 4 (left) and 6 (right).